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Fullerite with cavities containing dichlorobenzene (DCB) and isopropyl alcohol (IPA) molecules was prepared by the addition of IPA to a solution of fullerene C60 in DCB. On heating in vacuo fullerite evolves IPA, and the temperature increase to 200—350 °C results in the evolution of acetone. No products of DCB conversion were observed. Possible products of the interaction of 60 with two IPA molecules...
Two methods are described for doping of fullerite C60 with molecular oxygen at a pressure of ∼104 Pa and at temperature 20–30 °C. It was found by mass spectrometry using oxygen 18O as dopant that a portion of molecular oxygen absorbed by the pre-decontaminated fullerite (first method) is removed as CO and CO2 at the heating temperature ≤200 °C. Doping during fullerite precipitation from the liquid...
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