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An antimony microelectrode was prepared by quenching a molten Sb–Sb2O3 mixture (2% Sb2O3). The local pH in the vicinity of a cathode evolving hydrogen gas was directly measured using the microelectrode. The local pH during electrolysis of KCl-glycine aqueous solutions was increased by proton consumption; however, the increment decreased with increasing concentrations of glycine, a buffering agent...
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