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An efficient route for the synthesis of two amphiphilic type I [3:3]‐hexakis adducts of C60 equipped with enantiopure cyclo‐monomalonate addends was explored. Studies on their self‐assembling behavior by TEM and SEM revealed that minor modification of the size and chemical nature of their glycol‐substituted monomalonate addends and, consequently, of the shape of these giant molecules significantly...
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