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The [ε‐PMoV8MoVI4O36(OH)4{LnIII(H2O)}4]5+ (Ln=La, Ce, Nd, Sm) polyoxocations, called εLn4, have been synthesized at room temperature as chloride salts soluble in water, MeOH, EtOH, and DMF. Rare‐earth metals can be exchanged, and 31P NMR spectroscopic studies have allowed a comparison of the affinity of the reduced {ε‐PMo12} core, thus showing that the LaIII ions have the highest affinity and that...
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