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A new family of turbostratically disordered misfit layered compounds (ferecrystals), (PbSe)1.16(TiSe2)n, is described with n values of 1, 2, 3 and 4. These compounds were synthesized using the modulated elemental reactant method (MER). The high-resolution transmission electron micrographs of these compounds clearly show rotational disorder in the constituent layers of these compounds. θ – 2θ x-ray...
A series of new compounds La x Co 4 Sb 12 with the skutterudite crystal structure, where 0<x<1, was prepared using modulated elemental reactants. The evolution of the reaction was followed using calorimetry and X-ray diffraction. The modulated elemental reactants were found to inter-diffuse at temperatures below 150 o C forming an amorphous reaction intermediate...
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