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Two homoleptic Re(I) complexes of ortho and para-carborane isocyanide ligands were prepared as the first examples of a new class of metal-based BNCT and BNCS agents. The target compounds were prepared in low yield through the reaction of [Re 2 (O 2 CPh) 4 Cl 2 ] and [Re 2 (OAc) 4 Cl 2 ] with 3-isocyano-1,2-dicarba-closo-dodecaborane and a para-carborane...
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