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The first α-phosphanyl amino acetic acids (phosphanyl glycines) with a chiral N-substituent 1a–g have been synthesized by one-pot three-component condensation of diphenylphosphane and enantiomerically pure primary amines of the type (L)- or (R)-R1R2CHNH2 with glyoxylic acid monohydrate in diethyl ether at room temperature. Crystals of the N-(1S)-phenylethyl derivative 1d·MeOH, grown from methanol,...
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