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Partial cation exchange of Mg2+ ions with Fe3+ ions employing solid Mg(OH)2 as precursor yielded an ordered layered double hydroxide of Mg and Fe in the presence of carbonate anions. Structure refinement revealed that the compound adopts the polytype structure 3R1 (space group R$\bar {3}$m, a = 3.108 Å, c = 23.08 Å) and does not show any signs of cation order. It crystallizes with a unique cation...
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