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Three new homoleptic lanthanide(III) tris(pivalamidinates), [tBuC(NiPr)2]3Ln (Ln = Ce (1), Eu (2), Tb (3)) were synthesized by reaction of anhydrous LnCl3 with 3 equivalents of in situ prepared Li[tBuC(NiPr)2] in THF. X‐ray structural analyses confirmed the presence of homoleptic, unsolvated tris(amidinates) in which the central Ln3+ ions are coordinated by three chelating pivalamidinate anions in...
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