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P‐type Ni(OH)2 has been combined with n‐type CdS nanorods and nanocrystals for enhanced photocatalytic property due to the p‐n junction. Though CdS nanosheets exhibit fast charge transfer and large superficial area, the decoration of Ni(OH)2 was rarely reported up to now. In this work, the photo‐deposition of Ni(OH)2 nanoparticles on CdS ultrathin nanoflakes was established for efficient photocatalytic...