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Using 1,1,2‐triphenylethane‐1,2‐diol, AgSbF6, and NOSbF6, two different carbonyl products of rearrangement were synthesized: neutral ketone compound 1,2,2‐triphenylethanone (1) from NOSbF6 and coordination complex of Ag ion and aldehyde product ([Ag·22]+SbF6–) from AgSbF6. Single crystal X‐ray analyses reveal the different structure generated by different salt. UV/Vis absorption spectra and calculation...
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