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The investigation on the synthesis of α‐C deuterated analogues of cyclosporin A (CsA) in N‐methylated amino acid residues was performed. The reaction based on our previous report (Bachor et al 2014 J Mass Spectrom 49, 43–49) proceeds in the presence of bases like TBD or MTBD at pH 13.4. The obtained results suggest the possibility of introduction of 3 deuterons, 2 at the α‐C of sarcosine, and 1 at...
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