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A novel formation mechanism according to the oxidative dehydrogenation of organics has been proposed for the low-temperature preparation of carbon-based nanomaterials. Several typical organics including ethanol, 1-butanol, p-cymene and liquid paraffin are used as precursors to react with ammonium persulfate (APS) in an autoclave, and carbon particles are obtained as a validation. The reaction characteristics...
A novel method is developed for low temperature synthesis of carbon encapsulated spherical Fe7S8, equiaxed Fe3O4 and spherical porous FeOOH nanocrystals with a core–shell structure via a solid–solid reaction of ferrocene with (NH4)2S2O8, (NH4)2Cr2O7 and NH4ClO4 in an autoclave, respectively. Samples were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy...
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