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Since 5‐Amino‐3‐nitro‐1H‐1,2,4‐triazole (ANTA) is known to be a thermally very stable secondary explosive, our goal in this contribution was the synthesis of thermally stable but more powerful energetic compounds based on ANTA. Hence, we utilized ANTA to synthesize 5‐nitramino‐3‐nitro‐1H‐1,2,4‐triazole (1) by nitration with a mixture of concentrated sulfuric acid and 100 % nitric acid. ANTA was also...
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