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In this study, to prevent manganese dissolution from an acid treatment during the extraction of lithium ions (Li+), silica (SiO2) was mixed mechanically with lithium manganese oxide (Li1.33Mn1.67O4, LMO) by a high-energy milling technique followed by calcination. The milling process ensured high-level chemical homogeneity of metal oxides. The amorphous SiO2 imparted stability to the LMO spinel structure...
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