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Multiblock structured glucan ethers are prepared for the first time by BF3·OEt2 promoted transglycosidation of two cellulose ether homopolymers. First, model studies are performed with equimolar mixtures of methyl cellulose (MC) and deuteromethyl cellulose (MC‐d3), varying the amount of Lewis acid and temperature. Reaction is monitored by 1H NMR spectroscopy and electrospray ionization mass spectrometry...
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