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By coupling a Pt‐catalyzed fluorogenic reaction with the Pt‐electrocatalyzed hydrogen‐oxidation reaction (HOR), we combine single‐molecule fluorescence microscopy with traditional electrochemical methods to study the real‐time deactivation kinetics of a Pt/C electrocatalyst at single‐particle level during electrocatalytic hydrogen‐oxidation reaction. The decay of the catalytic performance of Pt/C...
To understand the catalytic properties or roles of different types of surface atoms on metal nanocatalysts, the catalytic kinetics and dynamics of the different types of surface atoms (plane and edge) were revealed for the first time by a statistical quantitative deconvolution of observables obtained from traditional single‐molecule nanocatalysis of Pd nanocrystals.It was found that the edge and plane...
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