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The 14-membered O2S2-macrocycle L reacts with AgPF6 in acetonitrile/dichloromethane (1:1) to yield the cyclic, double S–Ag–S bridged complex, [Ag2L2(CH3CN)4](PF6)2 (2), in which each Ag(I) is bound to two exo-oriented S donors arising from different macrocycles to form a 12-membered, di-Ag metallacycle. Two PF6− ions form weak intramolecular contacts [Ag⋯F, 2.925(2)Å] between the Ag centres in a bridging...
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