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The way is open for the physical and chemical characterization and single‐crystal growth of the orthorhombic o′‐In2O3 polymorph. Orthorhombic In2O3 is synthesized from rhombohedral corundum‐type rh‐In2O3 under moderately high‐pressure and high‐temperature conditions (8–9 GPa, 600–1100 °C) followed by recovery to ambient pressure and temperature. The crystal‐structure data at ambient conditions confirm...
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