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A new water‐soluble complex, Re(CO)3(pterin)(H2O), was synthesized and characterized by 1H NMR and FTIR spectroscopy, and by a combination of three mass spectrometry techniques: MALDI, probe electrospray ionisation (PESI), and ESI. Because, unlike most metal‐pterin complexes, the ReI complex is quite soluble in water, appropriate single crystals could be obtained for structural X‐ray analysis. We...
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