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A well‐defined single‐site titanium‐modified montmorillonite (MMT) with only one geometric construction ((SiO)3–Ti–NMe2) was obtained in moderate conditions. Reaction of tetrakis(dimethylamido)titanium with hydroxylated MMT was conducted by surface organometallic chemistry technique, and the surface structure was characterized by in situ Fourier transform infrared spectroscopy, 13C cross polarization...
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