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TiO2 electrospun nanofibers (TiO2 ENNFs) were synthesized with titanium tetraisopropoxide as precursor by an electrospinning process and characterized by SEM, TEM, XRD, XPS, FT−IR, UV and FL. For the excellent properties of film formation, Nafion/TiO2 ENNFs modified electrode was constructed, which exhibited an excellent electrochemiluminescence (ECL) performance and stability while K2S2O8 as co‐reactant...
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