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A new iron–sulfur cluster compound, namely [(μ‐BNT)Fe2(CO)6] (A; BNT = (R)‐1,1′‐binaphthalene‐2,2′‐dithiol), was synthesized by self‐assembly of BNT with [Fe3(CO)12] and characterized using 1H NMR, 13C NMR, infrared spectra and elemental analysis. The H2 evolution activity of A was evaluated in a constructed homogeneous photocatalytic system by combining A as catalyst, xanthene dyes as photosensitizer...
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