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A robust aluminum‐based metal–organic framework (Al‐MOF) MIL‐120Al with 1D rhombic ultra‐microporous was reported. The nonpolar porous walls composed of para‐benzene rings with a comparable pore size to the kinetic diameter of methane allow it to exhibit a novel thermodynamic‐kinetic synergistic separation of CH4/N2 mixtures. The CH4 adsorption capacity was as high as 33.7 cm3/g (298 K, 1 bar), which...
Various adsorbents for CH4/N2 separation were developed to enrich low‐concentration coal‐mine methane. Most are hydrophilic and cannot treat moist coal‐mine methane. We report for the first time a microporous zeolitic imidazolate framework Co(dcIm)2 (TUT‐100) with superhydrophobic properties for CH4/N2 separation. The CH4 adsorption capacity and CH4/N2 selectivity were as high as 45.29 cm3/cm3 and...
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