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The crystalline orientation and phase distribution are two important parameters for high‐performance 2D perovskite solar cells. Therefore, it is essential to understand how the structure of spacer ligands influences the orientation and phase distribution of resulting 2D perovskite films. In this work, a new member of Dion–Jacobson (DJ) phase 2D perovskites based on trans‐1,4‐cyclohexanediamine (CHDA)...
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