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Novel mixed ligand monoliths (MLM) for capillary electrochromatography (CEC) of a wide range of solutes differing in both polarity and size were introduced. The MLM capillary columns were based on the different compositions of octadecyl acrylate (ODA) and 2‐naphthyl methacrylate (NAPM) monomers in the presence of trimethylolpropane trimethacrylate (TRIM) crosslinker and a ternary porogenic solvent...
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