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Glycosides and thioglycosides based on monosaccharides in reaction with benzaldehyde dimethylacetal or p-methoxybenzaldehyde dimethyl acetal undergo FeCl 3 -catalyzed (20mol%) regioselective 4,6-O-arylidenation producing the corresponding acetals in high yields. FeCl 3 also mediates acetalation of glycosides and thioglycosides of cellobiose, maltose, and lactose affording the corresponding...
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