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We report here the synthesis of several tripod‐shaped oligo(p‐phenylene)s with legs composed of three or four phenylene units. Each leg is end‐capped with an iodine atom or a TMS or carboxyl group, and an ethoxy group is present on the functional arm. The tripod containing methyl tri(ethylene glycol) side chains was designed for biological applications. The key step in the synthesis is the Pd‐catalyzed...
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