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It's electrifying! Electrochemical cross‐coupling of aryl compounds provides a one‐step approach to unsymmetrical biaryl compounds. A boron‐doped diamond electrode is used as the anode to oxidise the phenolic hydroxy group to a phenoxy radical, with 1,1,1,3,3,3‐hexafluoroisopropylalcohol (HFIP) and tetraalkylammonium methylsulfate used as the solvent and electrolyte. Since no reagents are required,...
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