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We report the syntheses and characterizations of low‐spin FeII complexes of hexadentate ligands poised for anion‐triggered spin‐state switching in polar solutions: [Fe(L5‐OH)](BF4)2 (1) and [Fe(L5‐ONHtBu)](BF4)2 (3), in which L5‐OH and L5‐ONHtBu are tripodal iminopyridine ligands that contain methanolic or tert‐butylamide functional groups, respectively, bound meta to the pyridyl N donor atom. Solid‐state...
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