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The ambiphilic and small‐bite‐angle diphosphanylborane ligands Ph2PCH(PPh2)CH2B(C8H14) (2) and Ph2PCH2CH[B(C8H14)]PPh2 (3) containing the Lewis acidic 9‐boranorbornyl group B(C8H14) have been prepared in one step by regioselective anti‐Markovnikov hydroborations of 1,1‐bis(diphenylphosphanyl)ethylene and 1,2‐bis(diphenylphosphanyl)ethylene with 9‐borabicyclo[3.3.1]nonane (9‐BBN) under relatively drastic...
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