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Two sets of samples of LiCo 1−x Ni x O 2 (0 ≤ x ≤ 1) in unquenched and quenched states have been synthesized by microwave dielectric heating. Lattice constants determined from powder XRD are found to vary with the composition. SEM/TEM micrographs of the samples have shown defined facets. The BET surface areas of quenched samples are higher than the unquenched samples....
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