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Chrysene and its bisbenzannulated homologue, naphtho[2,3‐c]tetraphene, were synthesized through a PtCl2‐catalyzed cyclization of alkynes, which also furnished corresponding biaryls subsequent to a Glaser coupling reaction of the starting alkynes. The optoelectronic properties of 5,5′‐bichrysenyl and 6,6′‐binaphtho[2,3‐c]tetraphene were compared to their chrysene‐based “monomers”. Oxidative cyclodehydrogenations...
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