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Although first synthesized in 1940, the X-ray crystal structure of carbamoyl fluoride, NH2COF, has until now remained unknown. [1] NH2COF crystallizes in the orthorhombic space group Ibam, is planar, and exhibits a short C-N bond length, 1.3168(13) Å, implying a significant degree of donation from the nitrogen lone pair. The structure features one molecule in the asymmetric unit and eight molecules...
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