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The first single-crystal X-ray diffraction study of tetrafluorinated monosaccharide derivatives is presented. Both α- and β-methyl 2,3-dideoxy-2,2,3,3-tetrafluoro-d-galactopyranoside anomers adopt the 4 C 1 conformation. The values for the C1–O1 and C1–O5 bond lengths and the O5–C1–O1–CH 3 dihedral angles are in line with what can be expected from the anomeric and exo-anomeric...
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