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In this work, we report and discuss on the use and limitations of the natural abundance deuterium two‐dimensional NMR spectroscopy in polypeptide chiral and achiral aligning media in the studies of homogenous triglycerides at 14.1 T. As illustrative examples, two triglycerides with short and long alkyl chains were investigated: the 1,3‐di(butanoyloxy)propan‐2‐yl butanoate or tributyrin (TB) and the...
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