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Quadrupolar oligothiophene chromophores composed of four to five thiophene rings with two terminal (E)‐dimesitylborylvinyl groups (4 V–5 V), and five thiophene rings with two terminal aryldimesitylboryl groups (5 B), as well as an analogue of 5 V with a central EDOT ring (5 VE), have been synthesized via Pd‐catalyzed cross‐coupling reactions in high yields (66–89 %). Crystal structures of 4 V, 5 B...
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