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The electrochemical intercalation of hexafluorophosphate anion into a graphite electrode has been studied in mixed solvents of ethylene carbonate (EC) and ethylmethyl carbonate (EMC). The suppression effect of EC and the favourable effect of EMC on hexafluorophosphate insertion into graphite in these electrolyte solutions have been verified by electrochemical tests, ex situ XRD and in situ Raman....
The electrochemical intercalation of hexafluorophosphate anion into a graphite positive electrode from methyl propionate (MP) has been investigated by conventional electrochemical techniques in conjunction with in situ Raman spectroscopy and ex situ X-ray diffraction. Graphite electrodes could deliver stable reversible specific capacities higher than 100mAhg−1 in MP-based solutions at room temperature...
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