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Photocatalytic CO2 reduction (CO2PR) into multi‐carbon products (especially C2H4) is a highly attractive route for global carbon cycle, however, which is seriously limited by sluggish C‐C coupling kinetics and competitive hydrogen evolution reaction (HER) and so on. Herein, the fabrication of a novel supramolecular assembly of NiAl‐Fe‐TCPP is reported by intercalating iron porphyrin (Fe‐TCPP) into...
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