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La2CoMnO6 are synthesized at different annealing temperature ranging from 600°C to 1300°C, marked as S600, S800, S1000 and S1300. S600 has the R-3c and the rest have the Pnma structure. The DTA curve exhibits two exothermic peaks, at 553°C for the phase formation and 905°C for the oxygen redistribution into the lattice. Deduced from xps, S1000 has the highest lattice oxygen. S1300 has one extra xps...
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