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By in situ reduction of Ag+ ions pre‐dispersed inside thermosensitive microspheres of poly[(N‐isopropylacrylamide)‐co‐(methacrylic acid)] (P(NIPAM‐co‐MAA)), a 3D copolymer‐supported network of silver nanoparticles is created and extensively characterized by surface‐enhanced Raman scattering (SERS). The effective dispersion and the suitable density of the silver nanoparticles in the composite microspheres...
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