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We report a metal‐organic framework (MOF) supported monoligated phosphine‐cobalt complex, which is an active heterogeneous catalyst for aromatic C−H borylation and alkene hydroboration. The mono(phosphine)‐Co catalyst (MOF−P−Co) was prepared by metalation of a porous triarylphosphine‐functionalized MOF (MOF−P) with CoCl2 followed by activation with NaEt3BH. The MOF catalyst has a broad substrate scope...
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