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This work aimed to render phenomenologically autonomous the otherwise stepwise operation of a catenane‐based molecular switch, which is chemically triggered by the decarboxylation of 2‐cyano‐2‐phenylpropanoic acid (2). Given that any amount of 2 in stoichiometric excess with respect to the catenane is consumed in a side reaction, the authors resorted to the corresponding anhydride 5, the slow hydrolysis...
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