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A facile AlCl3‐mediated Friedel–Craft alkylation between a multi‐substituted benzyl bromide and benzene is established, in which a wide set of poly(phenylene methylenes) (MMSs) are synthesized through a two‐step strategy under metal‐free conditions with high yields (slightly lower than theoretical yields). The resulting MMSs, characterized by Fourier transform infrared spectrometry, nuclear magnetic...
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