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The first synthesis of hierarchical porous metal–organic frameworks (HP‐MOFs) is reported through a solvent evaporation‐induced co‐assembly of polystyrene‐block‐poly(ethylene oxide) (PS‐b‐PEO) and MOF building blocks. The growth of MOFs is restricted to confined spaces formed by self‐assembled PS‐b‐PEO, and mesopores and/or macropores are created after removing PS‐b‐PEO by solvent rinsing. This approach...
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