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The reaction of [Zr(TrenDMBS)(Cl)] [Zr1; TrenDMBS=N(CH2CH2NSiMe2But)3] with NaPH2 gave the terminal parent phosphanide complex [Zr(TrenDMBS)(PH2)] [Zr2; Zr−P=2.690(2) Å]. Treatment of Zr2 with one equivalent of KCH2C6H5 and two equivalents of benzo‐15‐crown‐5 ether (B15C5) afforded an unprecedented example (outside of matrix isolation) of a structurally authenticated transition‐metal terminal parent...
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