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Enantioselective copper‐catalyzed ring‐opening allylic alkylation of a cyclopropanol with an allyl phosphate was developed using a phenol‐NHC chiral ligand. DFT calculations indicated that a copper homoenolate is formed via Li−Cu bimetallic activation of a cyclopropoxide and that syn‐SN2’ attack of the Cu center of the homoenolate to the allyl phosphate followed by facile C−C bond formation affords...
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