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Topochemical reactions have led to great progress in the discovery of new metastable compounds with novel chemical and physical properties. With these reactions, the overall crystal structure of the host material is generally maintained. Here we report a topochemical synthesis of a hexagonal nitride hydride, h‐Ca3CrN3H, by heating an orthorhombic nitride, o‐Ca3CrN3, under hydrogen at 673 K, accompanied...
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