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A series of alkali metal 1‐adamantoxide (OAd1) complexes of formula [M(OAd1)(HOAd1)2], where M=Li, Na or K, were synthesised by reduction of 1‐adamantanol with excess of the alkali metal. The syntheses indicated that only one out of every three HOAd1 molecules was reduced. An X‐ray diffraction study of the sodium derivative shows that the complex features two unreduced HOAd1 donors as well as the...
A series of alkali metal 1‐adamantoxide (OAd1) complexes of formula [M(OAd1)(HOAd1)2], where M=Li, Na or K, were synthesised by reduction of 1‐adamantanol with excess of the alkali metal. The syntheses indicated that only one out of every three HOAd1 molecules was reduced. An X‐ray diffraction study of the sodium derivative shows that the complex features two unreduced HOAd1 donors as well as the...
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