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Efficient methods for functionalization of readily available exo‐glycals have been developed. Sequential palladium‐catalysed cross‐coupling of dibromo‐substituted exo‐glycals was first explored and allowed the formation of new disubstituted exo‐glycals as single stereoisomers. Bromination of furano‐ and pyrano‐methoxycarbonyl‐exo‐glycals led to a new series of monobrominated derivatives. These vinylic...
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